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The Effect of the Parameters of T-RTM on the Properties of Polyamide 6 Prepared by in Situ Polymerization

With the rapid development of the automotive industry, there is also a significant need to improve the raw materials used. Therefore, the demand is increasing for polymer composites with a focus on mass reduction and recyclability. Thermoplastic polymers are preferred because of their recyclability. As the automotive industry requires mass production, they require a thermoplastic raw material that can impregnate the reinforcement in a short cycle time. The most suitable monomer for this purpose is caprolactam. It can be most efficiently processed with T-RTM (thermoplastic resin transfer molding) technology, during which polyamide 6 is produced from the low-viscosity monomer by anionic ring-opening (in situ) polymerization in a tempered mold with a sufficiently short cycle time. Manufacturing parameters, such as polymerization time and mold temperature, highly influence the morphological and mechanical properties of the product. In this paper, the properties of polyamide 6 produced by T-RTM are analyzed as a function of the production parameters. We determine the crystallinity and the residual monomer content of the samples and their effect on mechanical properties.

Publication date: 18/12/2019

Author: Orsolya Viktória Semperger

Reference: doi: 10.3390/ma13010004

MDPI (materials)

This project has been co-funded with the support of the LIFE financial instrument of the European Union [LIFE17 ENV/ES/000438] Life programme

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Last update: 2022-01-31